Robertson_jmi.12868.pdf (866.48 kB)
Focused ion beam preparation of microbeams for in situ mechanical analysis of electroplated nanotwinned copper with probe type indenters
journal contribution
posted on 2020-01-28, 12:05 authored by Stuart RobertsonStuart Robertson, Scott Doak, Fu-Long Sun, Zhi-Quan Liu, Changqing Liu, Zhaoxia ZhouZhaoxia ZhouA site‐specific xenon plasma focused ion beam preparation technique for microcantilever samples (1 μm ‐ 20 μm width and 1:10 aspect ratio) is presented. The novelty of the methodology is the use of a chunk lift‐out onto a clean silicon wafer to facilitate easy access of a low‐cost probe type indenter which provides bending force measurement. The lift‐out method allows sufficient room for the indenter and a line of sight for the electron beam to enable displacement measurement. An electroplated nanotwinned copper (NTC) was cut to a 3 × 3 × 25 μm micro‐beam and in‐situ mechanically tested using the developed technique. It demonstrated measured values of Youngs modulus of 78.7 ± 11 GPa and flow stress of 0.80 ± 0.05 GPa, which is within the ranges reported in the literature.
Funding
EPSRC EP/R032203/
EPSRC grant EP/P030599/1
History
School
- Aeronautical, Automotive, Chemical and Materials Engineering
- Mechanical, Electrical and Manufacturing Engineering
Department
- Materials
Published in
Journal of MicroscopyVolume
279Issue
3Pages
212-216Publisher
John Wiley & Sons Ltd on behalf of Royal Microscopical SocietyVersion
- VoR (Version of Record)
Rights holder
© The AuthorsPublisher statement
This is an Open Access Article. It is published by Wiley under the Creative Commons Attribution 4.0 International Licence (CC BY). Full details of this licence are available at: http://creativecommons.org/licenses/by/4.0/Acceptance date
2020-01-23Publication date
2020-02-18Copyright date
2020ISSN
0022-2720eISSN
1365-2818Publisher version
Language
- en