Thesis-1979-Fayad.pdf (3.99 MB)
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Differential pulse polarographic study of drug compounds

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thesis
posted on 10.01.2018, 11:22 by Nabil M.M. Fayad
The work discussed in this thesis is in three parts. The initial work carried out was to develop a differential pulse polarographic (DPP) method for the determination of disodium cromoglycate (INTAL) in human urine samples. The method eventually recommended involves an ion-pair extraction of the cromoglycate with tri-n-butylbenzylphosphonium chloride into chloroform. After evaporating the chloroform and dissolving the residue in a buffer solution, down to 0.5 μg INTAL per ml urine can be determined. The method has the distinct advantages of simplicity and speed over the colorimetric method currently in use. [Continues.]

History

School

  • Science

Department

  • Chemistry

Publisher

© Nabil Mohamed Mohamed Fayad

Publisher statement

This work is made available according to the conditions of the Creative Commons Attribution-NonCommercial-NoDerivatives 2.5 Generic (CC BY-NC-ND 2.5) licence. Full details of this licence are available at: http://creativecommons.org/licenses/by-nc-nd/2.5/

Publication date

1979

Notes

A Doctoral Thesis. Submitted in partial fulfilment of the requirements for the award of Doctor of Philosophy at Loughborough University.

Language

en

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